Gain great flexibility with an intelligent collection concept

SpeedEx_Solutions_Flexible_rac_79f0a31c1d

By: Susanne Feifel

When it comes to ultra-trace analysis larger sample amounts are required to reach lower detection limits. Typical examples are ultra-trace analysis of food samples with a demand for representative sample amounts, e.g. food contact materials penetrating into food, or dioxins/furans determined in poly urethane foam being used for air monitoring tasks of living rooms or industrial facilities. Whenever solvent amounts of more than 150 mL per samples are collected, evaporation with the standard 220 or 240 mL collection vessel may be limiting.

With SpeedExtractor’s flexible collection concept you are able to accommodate a selection of different collection vessels which allow for transfer free evaporation and concentration of extracts.

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Application Note #64: Determination of Pesticides in Spices By Extraction

Determination of Pesticides in Spices

Determination of Pesticides in Spices

Application Note #64 describes a fast and reliable way to extract organochlorine and other pesticides in chilli and paprika spice samples with the SpeedExtractor E-916. After the extraction the extract was cleaned up via GPC and analyzed by GC-MS/MS. Contact us to request this Application Note.

Introduction:
A pesticide is any substance or mixture of substances intended for preventing, destroying, repelling or mitigating any pest. Pesticides can be classified by their chemical structure (organochlorines, organophosphates and carbamates) or by their target (herbicides, insecticides, fungicides, rodenticides, pediculocides and biocides).

The adverse health effects depend on the type of pesticide. Organophosphates and carbamates for example affect the nervous system. Others may irritate the skin or eyes. Some pesticides may be carcinogens. Others may affect the hormone or endocrine system in the body.

Experimental:
Instrumentation:
SpeedExtractor E-916 with 20 ml cells, GPC Gilson 233XL, Varian 3800 with MS-1200 QQQ

Samples:
Paprika and Chilli Powder with incurred pesticide content.

3 g sample was weighed in a beaker and 6 ml of water was added. The mixture was placed in the refrigerator over night. The next day 3 g of diatomaceous earth was added and mixed in well.

The sample was transferred into a 20 ml extraction cell. A fourfold extraction was carried out using the parameters shown within the Application Note. A blank and a spiked sample were extracted as well (QC test). After the extraction a GPC clean-up was performed and the pesticide content was analysed by GC-MS/MS. For comparison the samples were also extracted with a Dionex ASE® 200.

2011 ADSA-ASAS Conference Pictures

Here are several pictures from BUCHI’s booth at the 2011 ADSA-ASAS Conference held in New Orleans, LA this week. We’ve had alot of visitors and interest in our NIR, Kjeldahl and Extraction laboratory equipment and appreciate everyone who stopped by so far.

BUCHI Spring 2011 Newsletter

Welcome to our Spring 2011 Newsletter! You can view our entire laboratory equipment newsletter and read an overview below on the exciting things happening at BUCHI Corporation. Being a Buchi customer is a rewarding experience – from our world-class product quality to the ease of doing business with Buchi, the rewards are many. And now we are offering you the best kind of reward – savings in your pocket!

Stop by our booth #5300 at IFT 2011 this year and pick up your Customer Appreciation Voucher to SAVE 20% on the next Buchi instrument you purchase.

Latest News
2011 InterLabTec Award Winner! Our SpeedExtractor E-914/916 has recently received the InterLabTec-Award for outstanding achievements in “chemical-physical analysis”.
More Information on the SpeedExtractor Award

SelectScience 2010 Award: The NIRMaster was nominated for the Best Spectroscopy Product of 2010
More Information on the NIRMaster Nomination

New Products
The first stand-alone FT-NIR for Food and Feed industries: NIRMaster
This breakthrough instrument is the first stand-alone FT-NIR spectrometer which has been specifically designed with hygiene in mind for routing QC work in harsh environments in Food and Feed industries. Available in polymer and stainless steel housings, it includes a built-in PC loaded with a variety of ready-to-use calibrations.

Feature Products
Efficient and safe spray drying of aqueous and organic solutions with the B-290 Mini Spray Dryer

The B-290 is a bench-top system for quick and easy drying of aqueous solutions and suspensions, as well as organic solutions, with the optional Inert Loop B-295. This instrument is not only useful for feasibility studies, but also to produce small samples of dried product. Its easy operation facilitates obtaining optimized processes within a short time.

Minimize time between sample analysis and result generation with the SpeedExtractor

Despite modern extraction techniques, the process can be very time consuming. Thanks to the SpeedExtractor’s parallel format, up to six samples can be extracted simultaneously in approximately 20-40 minutes. As a result, incoming batches can be processed immediately and the analysis result made available on the same day, even if subsequent extensive purification steps are required. This allows for a previously unheard level of efficiency and throughput: up to 96 samples in one work day!

Upcoming Technical Webinars
Choosing the right solution for industrial scale evaporation, Wednesday, June 15, 2011, 1:30 PM EST
Click to register

By attending this webinar you will develop an understanding of what a complete evaporation solution looks like; how to accommodate typical environments and issues within industrial scale evaporation; and ways to easily and efficiently maximize your throughput.

Current trends in laboratory spray drying, Wednesday, July 27, 2011, 1:30 PM EST
Click to register

This webinar will provide a comprehensive overview of the most recent applications in laboratory spray drying, as well as illustrate how both the Mini Spray Dryer B-290 and the Nano Spray Dryer B-90 can be used to ensure application success.

Automated Chromatography overview featuring BUCHI Sepacore, Wednesday, August 17, 2011, 1:30 PM EST
Click to register

During this webinar we will focus on the complete BUCHI C-620 control package for the C-600 Sepacore system. We will review topics such as quick method set up, detailed complete data recording, manual control of the solvent pump, changing the gradient profile, and user interface configurable for touch screen operation.

BUCHI 7th Annual Technical Seminar & Workshop

BUCHI is hosting their 7th annual technical seminar and workshop today at the Holiday Inn in Somerset, NJ. Included here are some pictures at the event, please visit our website for any information on any of the laboratory equipment mentioned below.

BUCHI not only manufactures market leading instruments, but we also provide method development and application support to our customers. For more than 70 years, BUCHI has developed techniques and equipment designed to simplify your workflow and make your lab and facility more productive.

Attendees of this FREE one day seminar are learning essential technical information and participating in open discussions on implementation, application and method development among users and peers.

Agenda:
9:00 Registration with continental breakfast – Intro to BUCHI

9:15 BUCHI introduction and product overview

9:30 Sepacore® – Preparative and Flash Chromatography – Extended pressure range up to 725psi using innovative three piston pulsation free pumps – unmatched for Flash. Presented by Jeff Reid, BUCHI Corporation

•Benefits of a modular approach
•Various configurations, options, and setups
•SepacoreControl software and SepacoreRecord for data acquisition
•Unique Cartridger – high performing columns you can pack

10:15 Break

10:30 SpeedExtractor – Pressurized Solvent Extraction System, and Syncore® Concentration. Presented by William Ickes, BUCHI Corporation

•Design improvements simultaneously extract up to 6 samples in 20 minutes!
•Precise pressure and temperature control and reporting
•Unique design features for better reproducibility and accuracy
•Streamlined concentration with solvent recovery – Syncore and Multivapor™ together

11:15 Demonstration of Sepacore® and the SpeedExtractor. Open discussion and hands-on operation of instruments. Explore the flexibility of the Sepacore modular chromatography system and try samples on the world’s most innovative pressurized solvent extractor the SpeedExtractor.

12:00 Lunch – provided by BUCHI

1:00 Introduction to FTNIR and NIRCal®
Presented by Dr. Ron Rubinovitz, BUCHI Corporation

•Comparison of FTNIR to FTIR and Raman
•Pharma/Biotech – BUCHI’s unique fully validated ID library
•Nutraceuticals – Meet GMP requirements for incoming Material Identification
•Unique ChromaDex® Standards Data Base
•Steps for a successful NIR implementation

1:45 FTNIR – NEW developments
Presented by Dr. Ron Rubinovitz, BUCHI Corporation

•New NIRMaster Analyzer – World’s first “hardened” FTNIR – can be hosed down in process
•New software networking capabilities/continuous monitoring capabilities
•Checkmaster – Full automation at the Tablet Press – content uniformity and physical properties

2:30 Demonstration of N-500 FTNIR NIRFlex® Analyzer and NIRCal® Software. Open discussion and hands-on operation of instruments.

*The N-500 and the NIRMaster are in operation and a NIRCal software demo will be done this afternoon.